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Determination of Phosphorus Content & Gum Percent in Crude Edible Oil_A Complete Procedure 

MicroChem's Experiments
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22 окт 2024

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Комментарии : 88   
@deannedejella9782
@deannedejella9782 5 месяцев назад
This is a helpful procedure. Thank you! I'd like to as, can I use other buffer solutions instead of ammonia buffer?
@epalanisamiepalanisami6863
@epalanisamiepalanisami6863 3 года назад
Thank-you sir ,can you please explain, determinatiom of wax in sun flower oil by gravimetric method ?
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
Noted. Will make video later
@alkylpug
@alkylpug 3 года назад
This was very easy to follow, but can this procedure be used for ethanol as well? Cause I'm having a really hard time finding phosphorus content determination procedures for ethanol. It'd be a great help if you could answer ❤
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
No. This method is not applicable for ethanol.
@alkylpug
@alkylpug 3 года назад
@@MicroChemsExperiments Okay, thank you!
@seshuch8786
@seshuch8786 3 года назад
ThanQ so much for the procedure,phosphorous content method results are same as Spectroscopy method? ,i wnated to test for crude palm oil.
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
Yes, same. You can test in your lab and compare both results
@alstroemeria6626
@alstroemeria6626 3 года назад
Thank you for your great videos 🙏 could you upload a video about determination of metal ions in crude edible oil ?
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
Okay
@AliSfari
@AliSfari 2 месяца назад
Is it possible to calculate the amount of iron in edible oil using EDTA and how? Help me please
@AliSfari
@AliSfari 2 месяца назад
Can EDTA be used instead of disodium EDTA?
@schubertchilambe3602
@schubertchilambe3602 2 года назад
Thank you for sharing Few noticable things I would love to be clear about. 1. The temperature at which acetone and the sample is to be heated is not indicated 2. The buffer solution is also not indicated weather it is of 10pH or so . 3. And if possible I would love to understand where the 0.0313 x10⁶ is coming from and which type of oil is applicable to Thank you I will really appreciate
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
1. There is no specific temperature. Just boil the content at maybe 80 degree Celsius. 2. Buffer 10. 3. Same for all oils
@AliSfari
@AliSfari 2 месяца назад
Here we find the percentage of free phosphorus or what is present in the phosphatidyl compounds?    
@sparklingsoul8463
@sparklingsoul8463 11 месяцев назад
What is the ph for the ammonia buffer solution? 10?
@AliSfari
@AliSfari 2 месяца назад
Here we find the percentage of free phosphorus or what is present in the phosphatidyl compounds?
@AliSfari
@AliSfari Месяц назад
Please what reaction occurs in this test?
@prashant72002
@prashant72002 Год назад
This is process called Degumming of Vegetable Oils.
@UshanDeemanka
@UshanDeemanka Год назад
what is the temperature acetone need to be heated? according to a previous comment you have mentioned to 80C. bout acetone boiling point is 56C. is it okay to heat around 45C?
@MicroChemsExperiments
@MicroChemsExperiments Год назад
No matter of 80 degree or 56 degree. Just apply heat and stop when start boiling and remove the flask from heating mantle
@mherelalmonte4071
@mherelalmonte4071 2 года назад
@MicroChem's Experiments is this procedure is applicable in the determination of phosphorous content in RBD oil (Refined Bleach Deodorized Oil)?
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Yes. Applicable
@ernestogonzales800
@ernestogonzales800 2 года назад
The reference that you have cited at the beginning of the video does not indicate where the calculation factor of 0.0313 is taken from. Is there by any chance that you could tell me how this value was derived, or give me a link to a material that can maybe make the reason clearer why this is the value for the calculation factor? Thank you very much!
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
In reference, this method is not mentioned clearly. We develop this method internally using the basic of that reference.
@ernestogonzales800
@ernestogonzales800 2 года назад
was the formula that you used for phosphorus content based from the formula for percent chloridate titrated? it is the only formula from the reference book that i have found to be somewhat related, it is in page 205.
@suleimanmohammed1673
@suleimanmohammed1673 Год назад
were you able to know why he used that calculation factor? and can you please tell me the page of the book from which you found the reference
@methewskabungo2481
@methewskabungo2481 2 года назад
Hi what is the specific edible oil in the video and does that factor 0.0313 apply to all kinds of oil as in can I use it for sunflower soyabean or any other oil
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
It was crude soybean oil. Factor is the same for all kind of oils
@shahadatmazumder6776
@shahadatmazumder6776 2 года назад
It would be beneficial to share the Calcium Test of Limestone Grid and Calcium and Phosphorus Test of DCP, MCP Raw Materials. I am working as a laboratory chemist in a feed mill in Bangladesh.
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Okay we will develop
@allinsunilyadav4825
@allinsunilyadav4825 3 года назад
Thanks for video and keep it
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
Sunil Yadav, you are most welcome. Be with us.
@ovaneschakoyan7861
@ovaneschakoyan7861 2 года назад
What method is used for? AOCS or some other,please?
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Reference is given by at the very first of this video. Please play this video again and find the reference out
@sseshugiri1316
@sseshugiri1316 2 года назад
Is the result matches with spectrophotometer method result?
@chemistbd886
@chemistbd886 2 года назад
i think no
@suleimanmohammed1673
@suleimanmohammed1673 Год назад
@@chemistbd886 how do you determine it with spectrophotometer?
@thamerkadem3799
@thamerkadem3799 3 года назад
What is the reference for this method .. Thank you very much
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
Reference Method is mentioned in the first of this video. Please check it out.
@joshnabadgujar824
@joshnabadgujar824 Год назад
Does this method work if phosphorus content in oil is below 10ppm level?
@MicroChemsExperiments
@MicroChemsExperiments Год назад
Yes but in that case you have to use 0.001M EDTA solution during titration
@EarthChemEC
@EarthChemEC 2 года назад
please guide me method of gum determination through phosphoric acid
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Follow the method as described in this video
@ganeshpal6053
@ganeshpal6053 2 года назад
Please tell me the difference between spectrophotometer and this test
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Spectrophotometric test is more appropriate
@Jukchanning
@Jukchanning 4 года назад
thank you !!!
@MicroChemsExperiments
@MicroChemsExperiments 4 года назад
Sitti Mujur Channing Usman Duri, you are most welcome.
@Jukchanning
@Jukchanning 4 года назад
MicroChem's Experiments btw sorry for asking what is 0.313x10^6 stand for ??
@Jukchanning
@Jukchanning 4 года назад
may i know where you got that formula ?? please 😅
@MicroChemsExperiments
@MicroChemsExperiments 4 года назад
@@Jukchanning Please check the reference mentioned in the video title.
@MicroChemsExperiments
@MicroChemsExperiments 4 года назад
@@Jukchanning These are given by FAO to simplify the method.
@nohamahmoud2143
@nohamahmoud2143 3 года назад
I want to know Where did this result 25.5 and 0.0013 in the Equation of calculation of Phosphorus come from ?
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
These are calculation factors
@ahmedragabawaad2397
@ahmedragabawaad2397 2 года назад
[Factor 0.0313] ... This is atomic weight of phosphorus (31) devided by 1000 [The factor 25] ... This is convertion factor from phosphorus to phospholipid content
@mherelalmonte4071
@mherelalmonte4071 2 года назад
Ammonia solution and Ammonia buffer solution are the same?
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Yes. Same
@mherelalmonte4071
@mherelalmonte4071 10 месяцев назад
if I use Ammonia solution, what is the concentration allowed to use?
@basmaali5534
@basmaali5534 3 года назад
What is the initial volume reading, is it refer to blank?
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
It's the initial burette reading which we got before starting the titration.
@basmaali5534
@basmaali5534 3 года назад
@@MicroChemsExperiments if there is any experiment for sulfur content determination in oil available?
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
@@basmaali5534 Not yet. We will develop a video later. Stay with us.
@mayurkhedekar154
@mayurkhedekar154 2 года назад
Where I get details of this reaction ,name of this reaction?
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Not well known. You can study the reference given in the video title. Thank you.
@sankarsasi4925
@sankarsasi4925 2 года назад
How can determine calcium and magnesium in edible oil sir
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
You need to follow AAS method
@sankarsasi4925
@sankarsasi4925 2 года назад
spectrophotometer instrument not possible?
@chhoeunpeoumony6651
@chhoeunpeoumony6651 Год назад
what is 0.0313 x 1000000 stand for ? whtat is 25.5 number stand for ?
@MicroChemsExperiments
@MicroChemsExperiments Год назад
Factors
@mostafasalman2925
@mostafasalman2925 7 месяцев назад
Thx, Foctors‬‏ for what?
@nohamahmoud2143
@nohamahmoud2143 3 года назад
how can I calculate iodine value by colorimetry of vegetable oil ?
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
Sorry, we didn't make colorimetric video
@nohamahmoud2143
@nohamahmoud2143 3 года назад
​@@MicroChemsExperiments could you please explain it briefly here in the comment ? and also I want to know Where did this result 25.5 and 0.0013 in the Equation of calculation of Phosphorus come from ?
@justforentertainment74
@justforentertainment74 3 года назад
by wijs method
@chemistbd886
@chemistbd886 2 года назад
IF WE GOT SPECTROPHOTOMETRIC METHOD THEN WE WILL BE THANKFUL.
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
We will try
@suleimanmohammed1673
@suleimanmohammed1673 Год назад
@@MicroChemsExperiments for spectrophotometry method did you determine the concentration of phophates or phosphorous ? and if it was for phosphate did you use the conversion factor of 25.5?
@chemistbd886
@chemistbd886 2 года назад
This is very important video for soybean and rice bran oil, but it will be clear if you gave reaction mechanism with the experiment.
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Noted
@26-singhradhika94
@26-singhradhika94 3 года назад
What is the principal behind it
@MicroChemsExperiments
@MicroChemsExperiments 3 года назад
We will make video later explaining the principal
@hotsquarrel
@hotsquarrel 2 года назад
6:52
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
🙁
@Labtechnical2476
@Labtechnical2476 2 года назад
Please send method sr. No.... Like aocs or IS
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Sorry we dont provide any document
@AliSfari
@AliSfari 2 месяца назад
الو
@Labtechnical2476
@Labtechnical2476 2 года назад
Wrong method for soyabean oil
@MicroChemsExperiments
@MicroChemsExperiments 2 года назад
Ok
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