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How to remove high boiling solvent from crude- Reaction work up 

MH Chem
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23 сен 2024

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Комментарии : 19   
@fmdj
@fmdj 4 месяца назад
Oooh so *that* is what a rotovap is. I am pleased to see that - rotovap aside - my process for removing high boiling solvent from stuff is very similar, albeit much more messy.
@Dr.Mosharraf
@Dr.Mosharraf 4 месяца назад
😋😋😋
@bananthkumar3708
@bananthkumar3708 Год назад
I am one of your RU-vid follower , your videos was really very nice and helpful in my reaserch. Kindly make a video on how to make a crystals of carboethoxycyclopropyltriphenylphosphoniumtetrafluroborate. Sir if you make a video on this topic very helpful my reaserch work.
@Dr.Mosharraf
@Dr.Mosharraf Год назад
I will try
@vinitgaikwad7425
@vinitgaikwad7425 Год назад
Sir, do you recommend any source from where I can get to know all the possible azaeotropic mixtures of solvents
@Dr.Mosharraf
@Dr.Mosharraf Год назад
I will make a short video on that
@md.sydulislam4362
@md.sydulislam4362 Год назад
Kindly make a video about how to desalt any metal complex or ligand compounds/samples for HRMS characterization.
@ayanchakraborty2631
@ayanchakraborty2631 Год назад
You can try lyophilization with continuous washing
@md.sydulislam4362
@md.sydulislam4362 Год назад
@@ayanchakraborty2631 i tired with my Lyophilized sample. But it did not work. I used NaOH for pH adjustment, and the ligand has some bound hcl too.. Now after metallation reaction, I have lots of Na+ and Cl- that contained in the solid sample..
@ayanchakraborty2631
@ayanchakraborty2631 Год назад
@md.sydulislam4362, .if your metal complex is soluble in organic solvent, like DCM or Methanol then soluble it in 10% methanol in DCM filter the residue and evaporate the organic solvent to afford your desired metal complex..
@md.sydulislam4362
@md.sydulislam4362 Год назад
Thank you. I will try this.
@Dr.Mosharraf
@Dr.Mosharraf Год назад
I will try
@ayanchakraborty2631
@ayanchakraborty2631 Год назад
Kamon acho , dada??
@Dr.Mosharraf
@Dr.Mosharraf Год назад
Valo achi. Tumar Kemon cholche?
@ayanchakraborty2631
@ayanchakraborty2631 Год назад
@@Dr.Mosharraf.. Valo achi..Dada.. Post doc peyechi.. Taiwan a..
@Dr.Mosharraf
@Dr.Mosharraf Год назад
Great job
@ayanchakraborty2631
@ayanchakraborty2631 Год назад
@@Dr.Mosharraf tumi ki abar post doc join korle??
@Dr.Mosharraf
@Dr.Mosharraf Год назад
Na to. Ami industry te achi Ekhon
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