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Refining Gold Nuggets to Make a Standard Gold Test Solution 

Orophilia
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I inquart gold nuggets with silver and then dissolve out the impurities with nitric acid to make pure gold. I dissolve the pure gold in aqua regia to make three standard test solutions with varying concentrations. Finally, I test some ideas for measuring the concentration of samples using stannous chloride.
Keywords: inquart, inquartion, dissolving gold, aqua regia, stannous chloride, testing gold samples, gold concentration, gold mining.

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16 янв 2023

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Комментарии : 15   
@criscris5061
@criscris5061 Год назад
Wonderful 😅
@1kreature
@1kreature Год назад
If you looked closely at the bead after melting it, you had a combination of gold and silver, but it was by no means mixed properly. This will ruin the inquarting easily leaving the acid unable to "pick apart" some of the gold. These should show up later as larger lumps, or take very long time to be broken down.
@orophilia
@orophilia Год назад
Yeah, you're right. Some of the larger pieces took a very long time and I think I still had a bit of silver or base metals left in the gold. Gold prospecting is this weird and interesting experience. That's why I enjoy it so much. Thanks! -- Dave
@davevan1928
@davevan1928 Год назад
So what was the purpose of this video ? And is this gona be part of a series? The only reason I'm asking is you made 1.5 grams of silver and .36 grams of gold disappear.
@orophilia
@orophilia Год назад
:-) Yeah, it's magic how I made that gold and silver disappear. I recovered the silver by cementing it on copper and melting it into a bead, and the gold, I hope, is still in the fluid. I'm making standard solutions of known gold concentrations to be able to better quantify the amount of gold from ore samples, using SnCl2. Yes, it will become a series in the sense that I'll use the standard solutions to estimate gold concentrations in the ore, or at least that's the plan of the day. If it's not useful then I'll recover the gold and make a little bead. It's an enjoyable hobby. Thanks for the comment! -- Dave
@davevan1928
@davevan1928 Год назад
OK now the video makes sense to me. Ty sir
@douglaspohl1827
@douglaspohl1827 Год назад
Why not use your cellphone in a fixture since it can accurately measure over 15 million grey-scale values. Using Beer-Lambert law with known concentration you can create a gold concentration graph/slope line using dilutions standardized with x drop(s) of a detector solution like stannous chloride (SnCl2). Here is a RU-vid video to help. See: ru-vid.com/video/%D0%B2%D0%B8%D0%B4%D0%B5%D0%BE-1OLe98drl_c.html I recommend using spectrophotometer couvets. Good luck!
@orophilia
@orophilia Год назад
That's sort of the direction that I've been moving with this. I'd like a fast and easy test to roughly quantify the amount of gold. Thanks for the comment! Very useful. -- Dave
@douglaspohl1827
@douglaspohl1827 Год назад
@Orophilia Focus on best gold standards with excellent lab preparation... no spills or poor pipette. Maybe only 4 standards for field assay enough. I use 34.25 ppm gold = 1 troyoz/short ton ore. Good luck.
@orophilia
@orophilia Год назад
@@douglaspohl1827 I agree completely. I haven't been in a chemistry lab in 45 years and I'm very rusty. I'm trying to measure ~1 mg amounts of gold and I've got to work on good practices. Thanks! -- Dave
@orophilia
@orophilia Год назад
@@douglaspohl1827 Thanks so much. -- Dave
@myadventure7069
@myadventure7069 Год назад
Use potassium nitrate and newer overheat and then you don’t need respirator.
@orophilia
@orophilia Год назад
Yes, I've been watching your videos on this subject. Thanks so much. -- Dave
@myadventure7069
@myadventure7069 Год назад
I stop using nitric acide after my wife’s complains.
@orophilia
@orophilia Год назад
@@myadventure7069 Yes, it's a very nasty acid. I'm going to try KNO3. -- Dave
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