Тёмный

The Synthesis of 1,2,3,4-Tetrahydrocarbazole 

Corrosive Chemistry
Подписаться 5 тыс.
Просмотров 15 тыс.
50% 1

In this video I show the synthesis of tetrahydrocarbazole from phenylhydrazine and cyclohexanone using the Fischer indole synthesis.
The product will be used in a later video and the yellow colouration is not of concern (though quite visually displeasing) as the melting point was satisfactory. The product could be recrystallized again in MeOH with activated charcoal to try and remove most of the colour.
My Patreon: / corrosion
Music: Clarinet Concerto in A major, K. 622 - III. Rondo, Allegro

Опубликовано:

 

23 сен 2024

Поделиться:

Ссылка:

Скачать:

Готовим ссылку...

Добавить в:

Мой плейлист
Посмотреть позже
Комментарии : 29   
@lambdabaryon
@lambdabaryon 4 года назад
Great vid!! The music is perfect
@BackMacSci
@BackMacSci 4 года назад
The frame at 6:28 is at a NileRed/ChemPlayer level of videography and I want everyone to appreciate it. That is all. Also great channel!
@cvspvr
@cvspvr Год назад
rip chemplayer
@longnguyenhoang9608
@longnguyenhoang9608 4 года назад
Love this guy who made this video. I work in a research synthetic lab but dont have a chance to synthesize these simple compound.
@chimiokb
@chimiokb 4 месяца назад
Hello!In the last step at 9:36 there is a dehydrogenation reaction with Pb3O4. Do you have a citation for this reaction?
@firehoax9230
@firehoax9230 4 года назад
wtf why are your videos so good
@punitkumar8176
@punitkumar8176 4 года назад
Great video sir. I have done this same reaction using microwave for my master's project.
@DavidRobertsonUK
@DavidRobertsonUK 4 года назад
Really enjoyed this, thank you!
@abubakaranwar7038
@abubakaranwar7038 Год назад
When to add phenyl hydrazine before starting the reflux or after starting the reflux? Please reply me as soon as possible.
@Aragmatiki
@Aragmatiki 2 года назад
nicely done mate. I like your synth videos
@nareshbarik5384
@nareshbarik5384 7 месяцев назад
Thank u ❤
@simranpusatkar4000
@simranpusatkar4000 4 года назад
hey can this reaction be performed in photochemical conditions??
@mairisberzins8677
@mairisberzins8677 2 года назад
No, Fscher Indole synthesis required acidic environment for catalysed hydrogen transfers. Without that the reaction would be far too slow.
@sodaxuan7880
@sodaxuan7880 3 года назад
Just wondering, why does the solution turn dark brown when it is cooled down?
@karthi6990
@karthi6990 2 года назад
what happens if phenylhydrazine HCL salt form is used instead of free phenylhydrazine?
@kimyauzerine
@kimyauzerine День назад
Since hydrazine compounds are toxic, they are stored as salt in crystal structure. Adding NaoH here eliminates the HCl that provides the crystal structure.
@zacharyleduc1053
@zacharyleduc1053 4 года назад
Congrats! Awesome video! :)
@austin543_8
@austin543_8 4 года назад
Damn I'm jealous of your video quality
@atifmustafa2495
@atifmustafa2495 3 года назад
Amazing!! Thanks!😊
@patrickstar7693
@patrickstar7693 2 года назад
so how does it smell
@missionsuccess6323
@missionsuccess6323 Год назад
. Synthesis of 2-Amino-4-(substituted-phenyl)-1, 3-thi- azole Derivatives
@antifreeze-30degrees49
@antifreeze-30degrees49 Год назад
Reduce Fluorenone to Fluorenol by using non-toxic aluminum galinstan amalgam in ethanol solution.
@yavuzcelik1354
@yavuzcelik1354 2 года назад
Hi thanks your vidoes. Can you doing this syntesis.? 2, 4-bis [N-Butyl-N-(1-cyclohexyloxy-2, 2, 6, 6-tetramethylpiperidin-4-yl) amino]-6-(2- hydroxyethylamine)-1, 3, 5-triazine
@didimohammedelg5023
@didimohammedelg5023 Год назад
Can you send me the resource
@benzen3179
@benzen3179 3 года назад
9:03 what is the thermometer model
@corrosion-chem
@corrosion-chem 3 года назад
TM-902C K Type Thermometer I ordered on ebay
@jasminpansuriya6119
@jasminpansuriya6119 4 года назад
Sir recrylization from?? Napthenol
@jacobtierney4419
@jacobtierney4419 3 года назад
Methanol
@hensroth
@hensroth 2 года назад
The wet crude product kind of looks like terrible oatmeal
Далее
Simple Aniline Synthesis from Vitamin B10
9:56
Просмотров 8 тыс.
Triphenylbismuth Synthesis
21:45
Просмотров 16 тыс.
Распаковка iPhone 16 Pro Max
01:01
Просмотров 2,6 млн
«По каверочку» х МУЗЛОФТ❤️
00:21
Synthesis of 1,4-Dibromobutane from THF
10:33
Просмотров 8 тыс.
Alkylation of Cyclohexanone
16:00
Просмотров 43 тыс.
Making Tryptamines for Enlightenment
11:01
Просмотров 209 тыс.
Making Chromyl Chloride
15:06
Просмотров 235 тыс.
New Molecules for Chemistry with LEDs
13:33
Просмотров 44 тыс.
Making Liquid Nitrogen From Scratch!
13:43
Просмотров 8 млн
Making 4,N,N-Trimethylaniline - Super Glue Activator
12:45
From Rock to Copper Metal
15:37
Просмотров 2,7 млн
Making Rocket Fuel by Mixing Bleach & Ammonia
18:54
Просмотров 35 тыс.
Knorr Pyrrole Synthesis of Knorr's Pyrrole
11:46
Просмотров 7 тыс.
Распаковка iPhone 16 Pro Max
01:01
Просмотров 2,6 млн