How long does it glows? I couldn't hear anything in the video. My speakers are damaged (just in case you gave that information already). Does it stays for a short time
Acetic anhydride is no precursor to heroin. It is used to acetylate morphine into heroin. The precursor is morphine and not acetic anhydride. A precursor is a substance that can easily be converted into another without having to go through a complete synthesis. I would love to see how you convert acetic anhydride into heroin without using morphine. 😳🤪
Why are you making everything so complicated? Phosphorus pentoxide + H2SO4 = Sulfur trioxide as shown by "Random Experiments Int." in his youtube video "How to make sulfur trioxide". Btw, sulfur trioxide forms crystals at RT and is solid. Your sulfur trioxide is contaminated with a lot of phosphoric acid an therefor liquide.
What's the point of adding water beforehand and then removing it later by fractional distillation? It is easier to leave out the water, measure the density after distillation and dilute to the azeotrope.
Did you remember to include water in your yield calcuation for boric acid because i got a yield of 45% using these numbers: Na₂B₄O₅(OH)₄]·8H₂O 381,37 g/mol , H3BO3 68,31 g/mol
But it's a nice idea to even outsource the cost of the brainwash and thus wich hunt to the people. So full of manure. Btw. von der Leyen allegedly origianted from a family of betrayers and thiefs and.. she may have visited me in my dreams in 2021.. but I thought then it was a disguise and this disguise trick has happened a few times allready with other people. It was like this: I was in my home and it was haunted and the flat shrunk 3 times and I walked arround. At the end I've seen from one room a veil (actually a bed cover) just passing i.e. hinting that I've just missed to see that person who is wearing it. Sturdy as I am, I followed it into my sleeping room and there where my bed was, were stairs that lead into the lower levels and.. she was walking down and looked angry/cold in my eyes. I've seen the dark in her pupils. I guess it was supposed to look like that. Now, what happened at the time afterwards? The darkness in me was roughly about in it's ending but not completely. I really can't tell much more than this, it's a report at best.
Just make sure that you wear your standard PPE (lab coat ,goggles, gloves, etc.) and also doing it in a very well ventilated area (fume hood if possible) and you can also wear a gas mask just to be extra safe.
@@stephshighvoltagelab I used to do it when my set-up was less sophisticated but I now do it in a room with a strong fan to vent out any harmful fumes. I recommend you to handle the oxalyl chloride outside if you don’t have a proper set-up yet.
@@EddieTheH sure you can acetylate anthranillic acid to make methaqualone and also you can use it with phenylacetic acid and a touch of stinky pyridine to make phenyl 2 proponone that makes almost exclusively German marching powder . It burns aswell but I wouldn’t advise using it to cook food with bit stingy on the eye!
I wonder if you could have just dried the boric acid + NaCl and grind it to powder. Add Mg and maybe borax as flux, then ignite. If that works (I think it will), it would save you some purification steps.
How do you make the hydride of Boron? Boron trioxide can react with fluorine to make Boron trifluoride(as far as I know, I ain't trying unless I have an immediate use) Could that be a pathway to making the hydride?
You mean diborane (B2H6)? Crude borane can be made by reacting magnesium boride with an acid. Magnesium boride is produced by doing the same reaction shown in this video but with a higher magnesium stochiometry. The process you mean is reacting BF3 with a hydride which produce diborane with higher purity. Diborane is also often made with NaBH4.
@@hantrio4327 so I'm not going to get to NaBH4 that way if the equilibrium goes the other way (dyslexia?).. diborane is a useful reducing agent, but definitely not something I want to sit on (attempt to store) Would the termite reaction with aluminium work just as good as the magnesium? By react with acid, I assume you mean the hx gas not an aqueous solution, yes? Or organic soluble acid? Ending up with aluminum borohydride would be ideal of course.
@@petevenuti7355 Is it your goal to NaBH4? Aluminium can be used instead of magnesium but then you need to add sulfur to the mix to sustain the reaction however aluminium has the advantage that it will react less with the formed boron so it will be purer. I was thinking about aqueous acids but I don't have any experience with this reaction, maybe it won't work.
I think Sodium/Mg can also be used to reduce boric oxide to elemental boron. And regarding boranes (B2H6 in particular) there are several ways to make it involves use of LiH with BCl3 we can go with other reducing agent like BCl3 with H2 /LiAlH4. With BF3 one can go with NaOH to produce DB. According to a literature it can also be blade using NaBH4 with I2.
Yeah you can't make a hydride without a hydride source or hydrogen gas at high temperature. This is generally true for all elements that can be hydrided.
Sodium ions caused the yellow flame, so you should distill your isopropyl nitrite and make sure you rinsed the distillation apparatus with distilled water and dried thoroughly before the distillation.
This is what the wiki article source says: _"To demonstrate the property of triboluminescence, the crystals should be well-formed, and it is vital that they be completely free of solvent. The triboluminescence is best demonstrated by placing several crystals of the compound between two watch glasses and gently grinding. The light emitted is readily observed in a darkened room."_ So, maybe recrystallization for bigger crystals, dry with little heat and crush in dark.
@@frostchem I can confirm that the crystals are triboluminescent, but the luminescence is very weak, you have to adapt the eye in a dark room. The light might not be sufficiently strong to be seen on a video recorded with a regular camera. Similar to when you crash sugar crystals. The light was not particularly blue, just bright (white) if I remember correctly.
My bad. I was a bit lazy to do the math for finding the percentage yield but I’ll put in the percentage yield now for the next syntheses I’m going to do.
@@frostchem It is very important information, with tells you did reaction went well or not. Do not be lazy in case of org chem, lazyness can be deadly :P
@@ejkozan I got similar yields to the literature for the phthalimide and anthranilic acid but I got a lower yield for the N-acetylanyhranilic acid which got a 90% yield
I doubt any idiots would be able to get the precursors in the first place. But yeah, it was probably better to include the mols of the chemicals and it would get the dumber idiots out since you have to convert mols to grams.
Hi, great video! I have recently made my own oxalyl chloride on my channel and have bought triethylamine with the plan to do this. I made some phenol from salicylic acid with the idea of chlorinating the phenol, I'm worried it will require a whole day of running a chlorine generator as I don't have a proper fume hood to deal with that much chlorine. Can I ask where you got your 246trichlorophenol and if it's available to buy anywhere for amateur chemists?
Thanks! I got my 2,4,6-TCP from a Chinese chemical company called Macklin. I know a local chemical supplier that helps me with purchasing and shipping the chemicals from China to Malaysia. I could pretty much buy anything from Macklin since the chem supplier has the rights to do so. I don't know if Macklin ships to a country like the U.S, and if it will even allow you to purchase something as a amateur chemist. I also found a pdf file of somebody who made 2,4,6-TCP from phenol and you unfortunately have to chlorinate the phenol for 2 days: www.xif.fr/uploads/TCP.pdf
I get all my glassware from an online platform called Lazada which is like Ebay. I think Lazada only ships to South East Asian countries so you might not be able to purchase something if you were living in, i'm assuming, the U.S. I'll give a link to the seller of all the glassware I bought from so you could take a look if you wanted to: www.lazada.com.my/sum-yau-nice/?from=wangpu&langFlag=en&page=2&pageTypeId=2&q=All-Products
@@chemistryofquestionablequa6252 Yes there is one. A nitrite salt with sodium bisulfate as shown by Nurdrage. Yield with twice the amount of sodium bisulfate 95%, concentration HNO3 75% The youtube video form NurdRage is called "Make Nitric Acid from Sodium Bisulfate and Sodium Nitrate"
The type of glass beaker I used is made out of boro-silicate glass which means that it is made out of silica and boron oxide. Phosphoric acid will react with these oxides at high temperatures of 200°C and above to make silicon phosphate and boron oxide which are the final products if everything had fully reacted and destroyed the glass.
The cheapest and easiest way I know as of now is the reaction of sulfur monochloride and anhydrous sodium acetate. This is a video showing the method: ru-vid.com/video/%D0%B2%D0%B8%D0%B4%D0%B5%D0%BE-OrZ5Oa9K1R0.html&ab_channel=LabCoatz . Sulfur chlorides are nasty and dangerous compounds so you should only attempt doing that method if you have proper precautions and safety.
Acetic anhydride is basically just 2 acetic acid molecules bonded together and all the water molecules are removed. It wouldn't make any sense if you were to make an anhydride by adding water to the substance.
@@kemalk-gt7cusulfur chlorides and sodium acetate is another route but sulfur chlorides smell ungodly bad. The 2 step method he's referring to is likely a ketene lamp, but ketene is insanely toxic.
