Hello Sir, please explain that for GC or HPLC method validation, how it is decided to prepare what levels concentrations for LOD & LOQ? what is determined first, LOD or LOQ? Please make it understand with example...🙏
Follow ich Q3D guidline,..conc range on the basis of give limit by ich guidline ,..if As limit 1.5 ppm ,..so what is ur 100 %,.. Limit*wt/ dilution,.consider ,. As limit 1.5 ppm ,.taken wt 0.5gm n dilution in 10 ml ,.so 1.5*0.5/10= 0.075 is ur 100%
