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Synthesis of ZnO nanoparticles by sol gel method 

NANOTECHNOLOGY
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This video shows how to synthesize ZnO nanoparticles by the sol-gel method,
For this purpose 2 g of zinc acetate dihydrate was dissolved with a 15 ml of distilled water and 8 g of sodium hydroxide was dissolved in a 10 ml of distilled water. The solutions were stirred.
Then the sodium hydroxide solution was added to the
solution of zinc acetate with a constant stirring. Then 100 ml of ethanol was added the solution containing both sodium hydroxide solution and zincacetate. After the reaction, and evaporation of solvents in oven white ZnO nano powder was formed.
For more information about the synthesis method please refer to the following articles:
www.sciencedir...
doi.org/10.108...
doi.org/10.108...
If you have any question please comment bellow
#sol_gel
#nanoparticles
#synthesis

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5 сен 2024

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Комментарии : 118   
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 2 года назад
See full course:www.udemy.com/course/materials-characterization-techniques/?referralCode=1B30CC92C1A1C158BC16 Join nanotechnology discussion group in telegram: t.me/Nanotechnology_chat
@hassanelgharbimasc.4192
@hassanelgharbimasc.4192 3 года назад
I am glad that i found your channel .. Most of papers that I download are for researchers from IRAN.
@irvingmarquez1106
@irvingmarquez1106 2 года назад
Thanks so much!!! its very interesting the technique, it could develope at home!!!
@hamidrezarezania6679
@hamidrezarezania6679 5 лет назад
Brief and very useful, thanks
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 5 лет назад
Thanks
@abbasshoukat7842
@abbasshoukat7842 4 года назад
It is very useful video. I have some questions. 1) When we will dissolve NaOH and Zn acetate in 15ml and 10ml distilled water, Only Stirring is required r heating is required? If heating is required then kindly what should be the temperature. 2) What will be the best time for stirring? When we will add ethanol in prepared solution, What will be temperature that time? I am waiting for your comment. Thanks..
@irvingmarquez1106
@irvingmarquez1106 2 месяца назад
Thanks so much for sharing!!!
@owlpharoah9634
@owlpharoah9634 Год назад
Please how do you make it form on a glass?
@omsingharjit
@omsingharjit 2 года назад
1:40 how can to solide containing solution ZnO (solid ) and other Na salt , can be evaporate to give only Zno instead of mixture of the both solid ?
@michaelfikiru2107
@michaelfikiru2107 Год назад
Hi! thanks. it is excellent video. what about drying muffle furnace?
@its_torjum
@its_torjum 17 дней назад
Mam for how long exact duration we should keep the beaker (containing soln) inside hot air oven and at what temp . 🙏 your single rply will be very much helpful in my research.
@Ali-hm2hh
@Ali-hm2hh 11 месяцев назад
How long is it in the oven and what is the temperature?
@baruah917
@baruah917 2 года назад
mem..what is concentration of Zinc aceted and NAOH ( eg like 2 Molality
@nisarahmad9703
@nisarahmad9703 4 года назад
Very Useful Ma'am!! Kindly make a video on ZnO@GO Nanocomposites. Thanks
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Ok, I will.
@nisarahmad9703
@nisarahmad9703 4 года назад
@@NANOTECHNOLOGY_Nanoscience Thank you so much
@omsingharjit
@omsingharjit 2 года назад
I never found it on RU-vid that What is the difference between Alfa a MnO2 and Betab MnO2 And how to easily identify and prepare it . Can you tell me or share me related video .
@Tang俊
@Tang俊 2 месяца назад
Why did I synthesize the nano-zinc oxide, stacked appearance yellow, how to synthesize the relatively white nano-zinc oxide
@quanbinhhuynh7766
@quanbinhhuynh7766 4 года назад
Does burette contain ethanol or contain ethanol and NaOH for titration?
@omsingharjit
@omsingharjit 2 года назад
Is it possible to make Zinc oxide naino wire using aqus chemical method ?
@soumengiri2266
@soumengiri2266 3 года назад
Thanks a lot..If I want to dope Mg (Source MgCl2) with atomic ratio Mg: Zn (2%) then what amount of MgCl2 will be taken ?
@chandrikachouhan5945
@chandrikachouhan5945 3 года назад
please upload nanoprecipitation method for the preparation of nanoparticles of any drugs.
@quanbinhhuynh7766
@quanbinhhuynh7766 4 года назад
I have a question. Is the process only drying without heating?Thanks
@shivasai8784
@shivasai8784 4 года назад
Nice Explanation madam super how prepare nanoparticles by using fruit and vegetables waste please help me madam
@bahrideghfel3845
@bahrideghfel3845 4 года назад
very useful, thanks could please give a method to elaborate cu doped Zno nanoparticles
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Hi, I've sent you an email.
@monicareddy8261
@monicareddy8261 4 года назад
@@NANOTECHNOLOGY_Nanoscience can I too know how to. Prepare Cu - ZnO nanoparticles? What should be the ph value if Hydrolised solution?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
@@monicareddy8261 Hi dear, please send me an email, my contact information is available on the "about" part of the channel.
@MuhammadSaqib-hb4bf
@MuhammadSaqib-hb4bf 9 месяцев назад
good
@DineshDinesh-vz9pw
@DineshDinesh-vz9pw 3 года назад
Very useful medam
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
Glad you liked it
@ibrahimnazemqader9153
@ibrahimnazemqader9153 Год назад
Great video
@lemmatirfie
@lemmatirfie 2 года назад
Thanks
@fayazsalema2186
@fayazsalema2186 4 года назад
What will purity of zinc oxide in zinc oxide nano particles which we get?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Hi, about 90 percent.
@fayazsalema2186
@fayazsalema2186 4 года назад
@@NANOTECHNOLOGY_Nanoscience Thanks for Ur reply can we use sodium carbonate instead of sodium hydroxide,and color of zinc oxide nano we get is it white in colour. If u can share Ur mail id as I want to more about zinc oxide.
@fayazsalema2186
@fayazsalema2186 3 года назад
we have to use ethanol ?and also active zinc oxide and nano zinc oxide are same..?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
@@fayazsalema2186 In this method, yeah it's necessary. I haven't heard about active ZnO.
@aasma1101
@aasma1101 3 года назад
WONDERFULL
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
Thank you
@mustafakhalil007
@mustafakhalil007 4 года назад
I may wrong, but i think its better to centrifuge the ZnO before dried it ?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
You can do that too. There are different methods for the synthesis of nanoparticles.
@fadurecipes
@fadurecipes 4 года назад
Ma'am during stirring what should be the temperature. And how long time it will take to form White prepitate??
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
The temperature of stirring is between 50-60 C. In the final step, a burette is filled with 100 ml of ethanol and tiltrate dropwise to the solution containing both sodium hydroxide solution and zinc acetate. The higher the time of titration, the smaller nanoparticles. I recommend more than 3 hours for titration.
@fadurecipes
@fadurecipes 4 года назад
@@NANOTECHNOLOGY_Nanoscience Thank you so much ma'am.
@jeevaraj2327
@jeevaraj2327 3 года назад
Thank you so much madam, it's interesting and motivating for beginners like me. Can you kindly do some videos on inorganic perovskite oxide synthesis........
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
Sure, we will.
@jeevaraj2327
@jeevaraj2327 3 года назад
@@NANOTECHNOLOGY_Nanoscience 😊😊😊
@gbhxn731
@gbhxn731 4 года назад
Thanks for this menthod ....but i read in google he disolve in propanol not water..i dont know why,can you explain why??
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Hi dear, I think for this case the solvent is not important. We used water, but alcohol can be used too.
@jaiho4058
@jaiho4058 4 года назад
Thank u for the video, what is the use of ethanol? Is it for critical drying?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Hi, yes, it is.
@SUNILKUMAR-qi4mj
@SUNILKUMAR-qi4mj 5 лет назад
Nice but short
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 5 лет назад
Thanks for your comment.
@mahienergy841
@mahienergy841 2 года назад
Thanks a lot
@user-on9cl3mc4j
@user-on9cl3mc4j 4 года назад
hello. i have two qeustion. 1. how many time does it take in oven 2. after I dry liquid in oven for 3hour , this powder can be answered ZnO powder?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Hello, 1. about 24 hours is okay 2. yeah, the white precipitate is ZnO nanopowder, if you have done the procedure correctly.
@dilkibat6938
@dilkibat6938 4 года назад
When ethanol will add drop wise through burette what will be the temperature?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
The temprature will be between 50-60 C.
@Mari_yana
@Mari_yana 3 года назад
Can we do it from zinc nitrate and sodium hydroxide? How much is the solution and temperature maintain?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
Yes, 50-60 degree centigrade.
@rotuafetricia8238
@rotuafetricia8238 3 года назад
Hi. What concentration did you make for the compound?
@susanaperez9405
@susanaperez9405 2 года назад
What kind of morphology do you have with this method?
@Mankindblooms
@Mankindblooms 2 года назад
Hello mam, How much NaOH do we wan to add for this preparation?
@natapinobolivar
@natapinobolivar 4 года назад
Thanks for this video. I have a question. Should I add the whole NaOH or just until reach pH=12? I added the NaOH and the solution become clear! Also, it is necessary temperature during this process? and how much ethanol should I added?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Thanks for your comment. You just need to adjust the pH between 9 and 11 and you'd better heat the solution while it's stirring.
@nancySIX
@nancySIX 4 года назад
@@NANOTECHNOLOGY_Nanoscience around what temperature do you heat it to.
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
@@nancySIX About 50-60 C is okay.
@sarmadabd1406
@sarmadabd1406 4 года назад
Thanks for this useful video but i need to know how long the reaction need? please tell me time periods for reaction and evaporation.
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Hydrolysis reaction took about 2 hours and in order to evaporate the solvents the hydrolyzed solution is heated for about 24 hours.
@sarmadabd1406
@sarmadabd1406 4 года назад
@@NANOTECHNOLOGY_Nanoscience thank you so much ❤️
@jaiho4058
@jaiho4058 4 года назад
@@NANOTECHNOLOGY_Nanoscience i have a question? Heated in what? For what temperature? Thank u
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
@@jaiho4058 Use oven and an ordinary temperature to vaporize the solvents.
@jaiho4058
@jaiho4058 4 года назад
@@NANOTECHNOLOGY_Nanoscience okay thank you so much maam
@abdullahikilacousman1749
@abdullahikilacousman1749 4 года назад
Hello, is the NaoH added drop wise or all at a time?, also is the ethanol (100ml) added drop wise and for how long should the stirring last? Can i use methanol instead of ethanol, Thank you
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Hi, add NaOH dropwise to adjust the pH 9-11. Stirring for 2 hours is okay. Yes, you can use methanol as a solvent.
@abdullahikilacousman1749
@abdullahikilacousman1749 4 года назад
@@NANOTECHNOLOGY_Nanoscience Thank you very much
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
@@abdullahikilacousman1749 yrwlcm
@sssk162
@sssk162 3 года назад
Mam can u please give the reference of this method..i need it urgently
@blueskieszero
@blueskieszero 4 года назад
Hello. I am trying to make transparent SiO2 hydrophobic thin film coating solution for application to various surfaces by wipe/spray method. Can anybody advise on how I start on this project. I have limited lab equipment.
@amirawalludin3751
@amirawalludin3751 3 года назад
Hi, it is very good info. Can I replace zinc acetate dihydrate with Zinc Chloride and sodium hydroxide with sodium carbonate. Then, evaporation in an oven is how long and what is the temperature range???
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
Hi, thanks for your comment. Please read the following article: jurnal.unej.ac.id/index.php/prosiding/article/view/4189
@khizarmushtaq8620
@khizarmushtaq8620 4 года назад
can anyone help me by telling me the materials/chemicals required to form nano-tungsten oxide dihydride using simple anodizing process? I'd be grateful. Thanks.
@maheenahmad7328
@maheenahmad7328 Год назад
No ethanol???
@bel8770
@bel8770 5 лет назад
Tienen algún correo electrónico? Buen video
@abbasshoukat7842
@abbasshoukat7842 4 года назад
Hi,,, I have seen your video. This is so much beneficial. Kindly provide me Fe nano particles Fe2O3 by sol gel method.
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Thank you for your comment.
@rodoxxs6134
@rodoxxs6134 3 года назад
Excelent video... Do You know about industrial Process for the production Of ZnO nanoparticles? I am subscribed to your channel
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
Hi, you should use methods such as ball milling and so on.
@rodoxxs6134
@rodoxxs6134 3 года назад
@@NANOTECHNOLOGY_Nanoscience thanks for your advice, we are in contact... :)
@fahadalajmi8641
@fahadalajmi8641 2 года назад
@@NANOTECHNOLOGY_Nanoscience ball mill is used to produce nano powder, Sol gel is used to produce nano particals.
@sssk162
@sssk162 3 года назад
Mam can u please give the reference of this method i need it immediately
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 3 года назад
Put your email here and I will contact you.
@sssk162
@sssk162 3 года назад
siddharththakur051@gmail.com
@sssk162
@sssk162 3 года назад
@@NANOTECHNOLOGY_Nanoscience thank you so much
@sssk162
@sssk162 3 года назад
@@NANOTECHNOLOGY_Nanoscience my email id siddharththakur051@gmail.com
@rifathasan-oi1rv
@rifathasan-oi1rv 2 года назад
Mam,can U please the reference article of this method, i need immediately
@osamaalsuleimani2517
@osamaalsuleimani2517 4 года назад
Why are you adding 100ml of Ethanol ???
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
Actually, adding Ethanol is not necessary.
@monicareddy8261
@monicareddy8261 4 года назад
What should be the temperature of the oven?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
80 centigrade degrees is okay.
@monicareddy8261
@monicareddy8261 4 года назад
@@NANOTECHNOLOGY_Nanoscienceshould we maintain some ph value of the solution to obtain nanoparticle before keeping it inside oven?
@NANOTECHNOLOGY_Nanoscience
@NANOTECHNOLOGY_Nanoscience 4 года назад
@@monicareddy8261 What do you mean?
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