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Making Fe3O4 Magnetic nanoparticles | How to make Iron Oxide magnetite Nanoparticles 

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Magnetic nano particles, how to make magnetic Fe3O4 by precipitation using ammonium hydroxide, MNP. In area of magnetic nanoparticles for drug delivery, magnetic nanoparticles review, magnetic nanoparticles synthesis, magnetic nanoparticles applications, magnetic nanoparticles for cancer therapy How to make Iron Oxide magnetite Nanoparticles ? By this method Magnetite Fe3O4 nano particles obtained narrow size distribution about 40 nm. It can be used many area such as hyperthermia, MR imaging.

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5 сен 2024

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Комментарии : 94   
@khweziphumelelekalipa4056
@khweziphumelelekalipa4056 10 месяцев назад
Sr I have tried your method and it worked well, but I used 4.7g of FeCl3.6H2O and 4.0 of Fe2SO4.7H2O then i titrated with 6M NH4OH drop wise. then it takes 40 min to obtain FE3O4 naniparticles. Thank you
@mehnazparveen5277
@mehnazparveen5277 7 месяцев назад
How did you separate the particles? I've made too but now how will I separate the particles from the water?
@anurag5768
@anurag5768 6 месяцев назад
@@mehnazparveen5277 you can do centrifugation or filtration
@GingY9696
@GingY9696 10 дней назад
​@@mehnazparveen5277filter?
@keltoumromaissa2632
@keltoumromaissa2632 3 года назад
Please have you an article about this?
@aikonlatigid
@aikonlatigid 3 года назад
I uses electrolysis with 70 degrees centigrade caustic soda solution with iron as +electrode
@XCeedSaid
@XCeedSaid 3 года назад
Good one thank you 👍
@dogodogo5891
@dogodogo5891 3 года назад
ada ref pak?
@imochabi
@imochabi Год назад
Can you please tell me how long is the reaction time
@RBJSHETTY
@RBJSHETTY 4 месяца назад
Nice Video
@jozefnovak7750
@jozefnovak7750 Год назад
Super! Thank you very much!
@polymerscope6881
@polymerscope6881 Год назад
Thanks.
@rb9875
@rb9875 8 месяцев назад
merhabalar, fecl3ve fe2(so4).7h20 nun net rakamlarını yazı olarak yazabilirmisiniz. ilk etapta bunları suda çözdükten sonra nh4oh ı ne kadarlık seyreltik damla damla ekliyorunuz ben tam olarak anlayamadım video da. teşekkürler
@mariotorresflores3192
@mariotorresflores3192 2 года назад
This method doesn’t need nittogen bubling?
@kacgibibiter6640
@kacgibibiter6640 Год назад
Hocam merhabalar, Fe304'ü Türkiye'de bulabiliyor muyuz hazır olarak yoksa labda ayrıca hazırlamamız gerkeiyor mu? lisans öğrencisiyim bioadsorbentleri magnetize etmek için kullanmam gerekecek. İyi çalışmalar dilerim.
@polymerscope6881
@polymerscope6881 Год назад
Tabi ticari olarak bulabilirsin.
@ntdkhoa67
@ntdkhoa67 Год назад
sir, thank you for the video i need your helps, i have 2 questions for you 1. how many degrees Celsius do u strir it? 2. do you store it in a nitrogen atmospheres? because Fe3O4 particles are easily oxidized in air condition. I hope your respone, many thanks, sir
@polymerscope6881
@polymerscope6881 Год назад
Its about 70 C, Yes u need nitrogen atmosphere
@shanikaprasadini586
@shanikaprasadini586 2 года назад
For producing magnetic hydrogel can we directly add hydrogel to this nanoparticle solution ?
@polymerscope6881
@polymerscope6881 2 года назад
Yes u can but magnetic particles in the hydrogel structure may not be homogeneous distribution. U should try impregnation of Fe3/Fe2 ions method. There is an example work in my channel.
@newtoniangaming4832
@newtoniangaming4832 3 года назад
Can we perform this same experiment by reducing the weight of the reagents proportionally???
@ch3rnobog988
@ch3rnobog988 2 года назад
Yes, you can.
@GNP3WP3W
@GNP3WP3W 3 года назад
ugh *Clutches chest* the fact that you used anhydrous Iron(III) chloride to make an aqueous solution irks my soul.
@polymerscope6881
@polymerscope6881 3 года назад
Bro ! I only have this.
@DaveFer
@DaveFer 2 года назад
LOL I feel your pain ... and I'm not even a chemist. ;)
@nurnabila2210
@nurnabila2210 3 года назад
hi can you list what instrument and apparatus that you used. Thank you
@polymerscope6881
@polymerscope6881 2 года назад
I will upload a detailed video about it soon.
@sohelpervas4821
@sohelpervas4821 7 месяцев назад
please sir make a video about making alfa Feooh.
@dayumiqbal2332
@dayumiqbal2332 Год назад
Can u please share the article or give me some suggestion how to Agno3 incorporate into hydrogel??
@polymerscope6881
@polymerscope6881 Год назад
U can impregnation like this; doi.org/10.1080/00914037.2017.1291513
@Anubhavachebol2004
@Anubhavachebol2004 Год назад
hello sir, Thank you for this video, Can you please tell me how you dry magnetic nanoparticles?..... Can we dry these nanoparticles at 60 degree Celcius?
@polymerscope6881
@polymerscope6881 Год назад
yes, u can in oven
@berihuhaftu3960
@berihuhaftu3960 Год назад
what are the reaction parameters, at what temperature have you used?
@polymerscope6881
@polymerscope6881 Год назад
0.02 M FeSO4 and 0.04 M FeCl3 in 400 ml water at 80 C. U can add the 0.1 M NH4OH solution on this solution by dropwise to pH10 around.
@muhammadsaadansari
@muhammadsaadansari Год назад
​@@polymerscope6881 Reference or doi please?
@saurabhshukla6048
@saurabhshukla6048 2 года назад
How much (volume) Ammonium Hydroxide solution was used? What was the molarity of Ammonium hydroxide solution? When did you stop adding Ammonium Hydroxide? What if we use green leaf extract instead of water?
@polymerscope6881
@polymerscope6881 2 года назад
8 times the mole of Fe ion is required. U can use 10 times. The green leaf extract is used for green synthesis. But the reaction efficiency decreases.
@iqrafalak7139
@iqrafalak7139 2 года назад
Can you please tell me about procedure in written form or any article?
@polymerscope6881
@polymerscope6881 2 года назад
U can find many studies in the literature. I will upload a detailed video about it soon.
@aayshapandey5170
@aayshapandey5170 Год назад
I which solvent you make the solution?@H2O ?
@gamelogy5029
@gamelogy5029 2 года назад
Kindly tell the ratio of ammonium hydroxide with distilled water, thanks
@polymerscope6881
@polymerscope6881 2 года назад
We need 8 times as many moles of OH- ions as the total Fe (Fe2+ and Fe 3+) ions. So, we need to add about 10 times.
@rosyjayaprakash5682
@rosyjayaprakash5682 2 года назад
Hello brother I have chosen fecl3.6h20 and Fecl2.4H2O and Nh3 using 1:2 ratio and dissolved in 60 ml distilled water but I got xrd values for Fe2O3 not for fe3o4 nanoparticles, wat can I do brother plz tell me any suggestion. Thank you
@polymerscope6881
@polymerscope6881 2 года назад
I will upload a detailed video about it soon.
@immadamir
@immadamir Год назад
Hello, I have tried synthesizing magnetite using the method you have shown in this video. However, I did not add the ammonia hydroxide drop wise, I immediately added it. Upon vigorous stirring, the ppt became black and I left the solution to settle. I then tested it with a magnet and they were magnetite ppt. My question: Since I added the NH4OH immediately, is there any chance that the ppt are pre-mature? I want to use the ppt as pigment and for some reason I am unable to get the desired quality.
@reeree2014
@reeree2014 Год назад
My guess is that adding all the ammonium hydroxide at once will produce larger spongey masses instead of discrete particles. Usually a surfactant such as sodium dodecyl sulfate (dishwashing soap may work) is added as well to reduce particle size as well.
@Felahliir
@Felahliir Год назад
Try using some kind of surfactant in your solution, this tends to make smaller more uniform crystals instead of amorphous growths
@jodscience3741
@jodscience3741 11 месяцев назад
I think you create a lot of ferric and ferrous hydroxide as a side reaction if you add ammonium hydroxide all at once instead of adding it drop wise.
@dogodogo5891
@dogodogo5891 2 года назад
did ammonium hydroxide can be replace by only naoh?
@polymerscope6881
@polymerscope6881 2 года назад
Yes
@moustaphamohamed4856
@moustaphamohamed4856 2 года назад
hello i want know it is one step method or two step method. thank you
@polymerscope6881
@polymerscope6881 2 года назад
İt is one step metod
@astiradinia1954
@astiradinia1954 2 года назад
Excuse me, if we use NaOH. How many concentration do we need?
@polymerscope6881
@polymerscope6881 2 года назад
U can use same concentration. I will upload a detailed video about it soon.
@amirmirtalaei8277
@amirmirtalaei8277 3 года назад
sorry; I didn't understand,how much fe(II) and fe(III)?
@saurabhshukla6048
@saurabhshukla6048 2 года назад
What was the molarity of FeCl3 and FeSo4 solutions?
@polymerscope6881
@polymerscope6881 2 года назад
0.04 and 0.02 respectively
@saurabhshukla6048
@saurabhshukla6048 2 года назад
@@polymerscope6881 Thanks. I prepared MNPs using plants extract. After drying, the particles leave brown marks on paper. is it alright? Can the MNPs get rusty?
@polymerscope6881
@polymerscope6881 2 года назад
@@saurabhshukla6048 Yes, it is probably MNP. If u can use the EDX, XRD analysis tehniques, u can chatarcterized it.
@laks318
@laks318 3 года назад
Hi... thanks for the video... i had tried the same method. On adding NaOH solution, at one point the reaction mixture started to get very thick indicating the formation of magnetite nanoparticles. Can we stop adding the reducing agent then? or do we have to continue adding the same?I used 0.2M FeCl2.6H20, 0.4 M FeCl3.6H20 and 3M NAOH solution...
@keltoumromaissa2632
@keltoumromaissa2632 3 года назад
Please, did u add the NAOH until th pH becomes equal to 10 or just whn u observe the thick solution?
@polymerscope6881
@polymerscope6881 2 года назад
I will upload a detailed video about it soon.
@amysarahbenjamin2348
@amysarahbenjamin2348 3 года назад
Have u not used heat of 80°during the precipitation reaction
@polymerscope6881
@polymerscope6881 3 года назад
No, it only room temperature but if u used high temperature, u can obtain more smaller nanoparticles.
@sidraparveen4157
@sidraparveen4157 2 года назад
Hi, Is Nitrogen atmosphere necessary here?
@abdullahaa9300
@abdullahaa9300 2 года назад
What is the size should be?
@polymerscope6881
@polymerscope6881 2 года назад
Its about 100 nm.
@bonsakoi7435
@bonsakoi7435 3 года назад
can this be used to remove phosphates from water
@polymerscope6881
@polymerscope6881 3 года назад
It can be used for purpose but their adsorption capacity is low. So, u can synthesis polymer-Fe3O4 nano particles for obtain good adsorban.
@bonsakoi7435
@bonsakoi7435 3 года назад
@@polymerscope6881 you lost me what's that lol
@mariotorresflores3192
@mariotorresflores3192 2 года назад
@@polymerscope6881I'm using sargassum as adsorbent ¿do you think it might work?
@hutsunprabhus8510
@hutsunprabhus8510 Год назад
Hi sir.... I have tried this method. After addition of NAOH and continuous stirring. I moved up a magnet over the sides the beaker ,the particles haven't risen up.... I am not sure about the amount and concentration of added NAOH...What might happened? can you pls tell sir...
@hutsunprabhus8510
@hutsunprabhus8510 Год назад
Also, what happen if I add excess NAOH? Pls reply sir ....
@polymerscope6881
@polymerscope6881 Год назад
The base concentration is very important. If it does not move, the reaction has not occurred. 8 times the mole of Fe ion is required. Fe3+ and Fe2+ use 0.04 M and 0.02 M respectively. U can try again by using NaOH dropwise until pH 10.
@hutsunprabhus8510
@hutsunprabhus8510 Год назад
@@polymerscope6881 sir can you pls tell the exact concentration and volume of NAOH that should be added to the concentration of the precursor that you have mentioned.
@hutsunprabhus8510
@hutsunprabhus8510 Год назад
@@polymerscope6881 Also can you pls tell the volume of FeSO4.7H2O(0.04M) and Fecl3.6H2O(0.02M) . I am not sure about it .pls reply sir
@sarahassan1824
@sarahassan1824 Год назад
@@hutsunprabhus8510 Did you get an answer ? Bec i will prepare with same chemicals
@rehamatya6704
@rehamatya6704 3 года назад
Is not necessary to perform this experiment under nitrogen?
@polymerscope6881
@polymerscope6881 2 года назад
Yes, it can be more correct.
@rosyjayaprakash5682
@rosyjayaprakash5682 3 года назад
Hello brother which compound r u using in tis synthesis
@polymerscope6881
@polymerscope6881 3 года назад
FeSO4 and FeCl3 (Fe2+ and Fe3+ mole ratio 1/2) used for Fe3O4 supply. To reduction reaction, NH3 aqueous solution used bur u can use another base solution such as NaOH aqueous solution.
@SatpalSingh-gg4kf
@SatpalSingh-gg4kf 2 года назад
how much ammonia consumed..
@polymerscope6881
@polymerscope6881 2 года назад
9 times as mole as total Fe ions
@weiwang1625
@weiwang1625 3 года назад
Please check the amount of the agent. the FeCl3 should not be 9.4g to keep the Fe3+/Fe2+ =2 to form Fe3O4?
@weiwang1625
@weiwang1625 3 года назад
Got it. sorry about this!
@anuragraut7002
@anuragraut7002 2 года назад
Which method use sir
@mariotorresflores3192
@mariotorresflores3192 2 года назад
It’s coprecipitation method
@krishnapatel0711
@krishnapatel0711 2 года назад
sir please send the research paper of this experiment......
@polymerscope6881
@polymerscope6881 2 года назад
I have not publish this experiment yet but u can find many studies about that in the literature
@rockymendusa7867
@rockymendusa7867 3 года назад
how to make this Fe3O4 have spike?
@miladnaeimi1514
@miladnaeimi1514 3 года назад
Gloves😳😳
@miladnaeimi1514
@miladnaeimi1514 3 года назад
PPE 😳😳
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